Parallel, Batch and Flow Reactions in a Temperature Controlled Environment

  • Multiple vial format options (0.3-700ml)
  • Temperature controlled with thermostatic fluid
  • Unparalleled light configuration and control
  • Interchangeable light modules with multiple wavelength options
  • Leverage up to 4 wavelengths simultaneously
  • Heavy Duty Magnetic stirring

Industry Leading Photoreactor Design

The LUCENT360™ is the most comprehensive photoreactor on the market. It’s patent pending design provides the most flexibility for parallel, large batch and flow photochemistry.

Reaction vials are immerged in a thermostatic bath controlled by an external heater/ chiller unit, enabling temperature controlled experiment conditions.

Light irradiation is provided by custom, interchangeable light modules that surround the reaction chamber.

The reaction chamber itself is comprised of 2 glass walls (Dewar) that thermally insulate light sources from the reaction vial bath.

Temperature Controlled

Reaction vials can be thermostatically controlled via a standard heater/chiller unit..

Interchangeable Light Modules

Four light modules surround the reaction chamber and one light module sits underneath.

Thermally Insulated Reactions

Double glass walls of the reaction chamber keep reaction vials at the correct temperature.

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Temperature Controlled Environment

The LUCENT360™ advanced photoreactor includes standard circulation ports on all of its vial holders as well as an internal water pump and high performance heat exchanger.

Connecting the LUCENT360™ to a standard heater/chiller unit enables accurate temperature controlled reaction conditions that are insulated from the heat of light modules. A temperature probe (included) can also connect to each of the LUCENT360 vial holders, allowing for precise measurements. Fill and flow rate is controlled by the manual valves accessed on the front panel.

Mutiple Reactor Vessels Enable Parallel, Batch or Flow Reactions

0.3ml x 24

4ml x 24

8ml x 24

20ml x 12

700mL Reactor

The 700ml reaction vial allows large batch photochemistry with the benefit of temperature controlled conditions.

Flow Reactor

Enables scaling of photochemistry reactions by significantly increasing surface area. Flow reactors are made of PFA tubing and are available in 20ml and 50 ml volumes.

Multi-light Screener

Our unique holder enables simultaneous light wavelength (or intensity) experiments that have been impossible until now.

Unparalleled Control of Light Wavelengths and Intensities

The LUCENT360™ includes 5 light modules that can be controlled independently. Each module has multiple LEDs that operate at a specific wavelength.

The light modules are interchangeable and, when using a divider in the reaction chamber, enables conditions that can screen multiple wavelengths or light intensities simultaneously.

Large Scale Experiment

LED #1: 100%
LED #2: 100%
LED #3: 100%
LED #4: 100%
LED #5: 100%
Small Scale Parallel Experiment

LED #1: 100%
LED #2: 100%
LED #3: 100%
LED #4: 100%
LED #5: 0%
Light Wavelength Screening

LED #1: 365nm
LED #2: 380nm
LED #3: 405nm
LED #4: 450nm
LED #5:
Light Intensity Screening

LED #1: 100%
LED #2: 80%
LED #3: 60%
LED #4: 40%
LED #5: 0%

Lucent360 Case Studies

Case Study: Scaling Up

A reaction was performed at 100 mL scale (5 mmol) with the Lucent360™ batch reactor (HCK1021-01-007) at 450 nm equipped with nitrogen inlet/outlet ports, a septum for syringing in reagents/sampling and a temperature probe. The reaction is cooled by an external chiller set at 25 °C. 

Case Study: Multiple LED Intensity Screening in a Single Experiment

The Lucent360™ allows you to quickly investigate the reactions parameters necessary to scale up a reaction at small scale with production using the same instrument. We used it to screen multiple light intensities in one experiment

Power measurement in Lucent360™

To measure the effective irradiation of samples in the Lucent360™, we performed actinometric experiments with several vial configurations.

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EvoluChem Lucent360 Advanced Photoreactor and Accessories List 2020

SKU / Product ID Item Description
HCK1021-01-020     Lucent360 Advanced Photoreactor STARTER package Lucent360 Advanced Photoreactor STARTER package includes:
1x Lucent 360 Advanced Photoreactor
1x Holder 4 ml vial
1x set of 450nm light modules (5 total)
HCK1021-01-021 Lucent360 Advanced Photoreactor
INTERMEDIATE package
Lucent360 Advanced Photoreactor
INTERMEDIATE package includes:
1x Lucent 360 Advanced Photoreactor
1x Holder 4 ml vial
1x Holder 20 ml vial
1x 4 ml screening holder
1x set of 365nm light modules (5 total)
1x set of 450nm light modules (5 total)
HCK1021-01-022 Lucent360 Advanced Photoreactor EXPERT Package Lucent360 Advanced Photoreactor EXPERT package includes:
1x Lucent 360 Advanced Photoreactor
1x Holder 0.3 ml vial
1x Holder 2 ml vial
1x Holder 4 ml vial
1x Holder 8 ml vial
1x Holder 20 ml vial
1x 700 ml photoreactor
1x 20 ml flow cell
1x 2 ml screening holder
1x 4 ml screening holder
1x 8 ml screening holder
1x set of 365nm light modules (5 total)
1x set of 380nm light modules (5 total)
1x set of 405nm light modules (5 total)
1x set of 450nm light modules (5 total)
HCK1021-01-023 Julabo Corio-CD 200F External Heater/chiller to control Lucent360 Advanced Photoreactor Temperature
HCK1021-01-001 Lucent360 Advanced Photoreactor Lucent 360 Advanced Photoreactor (no parts or accessories)
HCK1021-01-002 Lucent360 Holder 0.3 ml vial Holder for 48 x 0.3 ml vial 6 mm diameter
HCK1021-01-003 Lucent360 Holder 2 ml vial Holder for 24 x2 ml vial 12 mm diameter
HCK1021-01-004 Lucent360 Holder 4 ml vial Holder for 24 x 4 ml vial 15 mm diameter
HCK1021-01-005 Lucent360 Holder 8 ml vial Holder for 24 x 8 ml vial 17 mm diameter
HCK1021-01-006 Lucent360 Holder 20 ml vial Holder for 12 x 20 ml vial 28 mm diameter
HCK1021-01-007 Lucent360 700 ml Reactor Large format 700 ml reactor
HCK1021-01-008 Lucent360 20 ml Flow Cell (Reactor) PFA tubing, 20 ml Flow Reactor
HCK1021-01-009 Lucent360 2 ml Multi-screen Holder Multi-screen vial holder with 4 sections of 4 x 2 ml vial 12 mm diameter
HCK1021-01-010 Lucent360 4 ml Multi-screen Holder Multi-screen vial holder with 4 sections of 4 x 4 ml vial 15 mm diameter
HCK1021-01-011 Lucent360 8 ml Multi-screen Holder Multi-screen vial holder with 4 sections of 4 x 8 ml vial 17 mm diameter
HCK1021-01-012 Lucent360 Side LED 365 nm One (1) Side LED light module at 365 nm for Lucent 360
(Side LED modules are interchangeable)
HCK1021-01-013 Lucent360 Side LED 380 nm One (1) Side LED light module at 380 nm for Lucent 360
(Side LED modules are interchangeable)
HCK1021-01-014 Lucent360 Side LED 405 nm One (1) Side LED light module at 405 nm for Lucent 360
(Side LED modules are interchangeable)
HCK1021-01-015 Lucent360 Side LED 450 nm One (1) Side LED light module at 450 nm for Lucent 360
(Side LED modules are interchangeable)
HCK1021-01-016 Lucent360 Bottom LED 365 nm One (1) Bottom LED light module at 365 nm for Lucent 360
HCK1021-01-017 Lucent360 Bottom LED 380 nm One (1) Bottom LED light module at 380 nm for Lucent 360
HCK1021-01-018 Lucent360 Bottom LED 405 nm One (1) Bottom LED light module at 405 nm for Lucent 360
HCK1021-01-019 Lucent360 Bottom LED 450 nm One (1) Bottom LED light module at 450 nm for Lucent 360

 

 

 

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