
Suzuki Cross Coupling Array Standard Kit (HCK1003-01-001)
1 set of 6 catalysts (Pd(PPh3)4, Pd(
This kit requires EvoluChem reaction block (HCK1006-01-002) included in the EvoluChem Starter Kit (HCK1006-01-001)
The typical protocol is performed at 0.15 mol/l concentration reaction condition and
Protocol at 100 µl volume reaction condition
- Prepare
required volume of a 0.15 mol/L solution of combined substrates (boronic acid reagent and halogenated substrate) in the selected solvent. For example, 450 µl solution for 4 reaction conditions. - Using a clean and dry syringe, add 100 µl of substrates solution to a reaction vial and mix with the catalysts using the syringe.
- Add 30 µl of the selected base solution. (2 equivalents)
- Stir the reaction vials in the reaction block at
desired temperature (forexample: 80°C) for 3 to 12 hours. - Remove the vial caps using a
decapper . - Prepare
analytical sample for each reaction condition with 5 µl sample diluted into 200 µl in either DMSO or water/acetonitrile 50/50. Analyze resulting analytical samples by LC/MS.
Contact Us!
Interested in learning more about our products?
Complete our short contact form and we'll get back to you as soon as possible.
HepatoChem Inc
100 Cummings center, Suite 451C
Beverly, MA 01915 USA
office: +1 857 313 9508
fax: +1 617 274 0827
Info@hepatochem.com