Copper Catalyzed Amination Kit
The Copper catalyzed amination kits is the ideal tools for the investigation of Ullmann reaction conditions. This enables to conveniently screen multiple reaction conditions simultaneously using pre-weighed catalysts and reagents. We offer pre-selected arrays of precatalysts and salts or custom arrays depending on your needs.
- Copper Source: CuI
- Ligands: Phenanthroline, S-Proline, 1,2 cyclohexanediamine, N,N’dimethylethylenediamine, Isobutyrylcyclohexanone
- Base: K2CO3, Cs2CO3 and K3PO4
- Solvent: DMF, DMSO, dioxane or acetonitrile
- Temperature: 40°C -> 120°C
Standard Protocol: 50 µmol of substrates in 500 µl solvent (DMF, DMSO, dioxane or acetonitrile, 0.1 mol/L concentration) with 0.1 equivalent of CuI, 0.2 equivalent of ligand and 1.1 equivalent of base.
|CuI / Ligand|
|No Ligand||Phenanthroline||S-Proline||1,2-cyclohexane diamine||N,N′-Dimethyl ethylenediamine||Isobutyrylcyclohexanone|
6 catalyst systems & 3 bases
Kit contents: 2 reaction vials of each catalyst system and base, 36 reaction vials total
For more information contact us at firstname.lastname@example.org