Palladium & strong base kits

These kits are composed of 0.3 ml vials loaded with a catalyst and with a strong base in separated vials. The reagents are weighed individually and conditioned under inert condition. We offer a choice of arrays that allows to easily screen reaction conditions within few hours. Each included 2 set of reagents.

Catalysts and Bases Array

Catalysts and Bases Array

Available Palladium strong base arrays

 

HCK1004-01-003: 5 Catalysts and 2 bases in separated vials. (20 vials total)

HCK1004-01-005: 8 Catalysts and 3 bases in separated vials. (48 vials total)

HCK1004-01-014: 8 Catalysts and 2 bases in separated vials. (32 vials total)

 

Substrate 15 µmol Strong Bases 22.5 µmol (1.5 eq)
Precatalysts 1.5 µmol (10%) LHMDS NaOtBu P2-Et
BrettPhosG2

Primary array

 HCK1004-01-003

 5 catalysts & 2 bases

Extended array

 HCK1004-01-005

8 catalysts

&

3 bases

RuPhosG2
XPhosG2
tBuXPhosG3
tBuBrettG3
Pd2dba3/dppf

Extended array

 HCK1004-01-014

8 catalysts & 2 bases

Pd(PtBu3)2
Pd(OAc)2/CataCXium®

 

HCK1004-01-010: 8 Catalysts and 2 bases in separated vials. (32 vials total)

HCK1004-01-011: 8 Catalysts and 3 bases in separated vials. (48 vials total)

HCK1004-01-012: 8 Catalysts and 2 bases in separated vials. (32 vials total)

HCK1004-01-013: 8 Catalysts and 3 bases in separated vials. (48 vials total)

 

Substrate 15 µmol Strong Bases 22.5 µmol (1.5 eq)
Precatalysts 1.5 µmol (10%) LHMDS NaOtBu P2-Et
BrettPhosG2

Primary array

 HCK1004-01-010

8 catalysts & 2 bases

Extended array

 HCK1004-01-011

8 catalysts

&

3 bases

RuPhosG2
XPhosG2
tBuXPhosG3
tBuBrettG3
AmphosG3
AdBrettPhosG3
CataCXium® A G3
DavePhosG3

Primary array

 HCK1004-01-012

8 catalysts & 2 bases

Extended array

 HCK1004-01-013

8 catalysts

&

3 bases

JackiePhosG3
JosiPhosG3
P(t-Bu)3G4
PCy3G4
RockPhosG3
SPhosG3
XantPhosG3

 Protocol:

 

pdstrongbaseprocess